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Under-dilution (too little water) raises peptide concentration above solubility thresholds, causing precipitation you won't see until week two
Bulletin of Experimental Biology and Medicine, 133 , 614-616
Experimental data indicate increased functional tone of the lower esophageal and pyloric sphincters following peptide administration, a response associated with reduced reflux-related injury and attenuation of esophageal inflammation in animal models (11)
Using expired b12 could certainly result in you not receiving the proper dosage due to deterioration as you now likely suspect given your setback
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